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SediGraph III Plus, Micromeritics technology

Malvern Panalytical

SediGraph III Plus, a Micromeritics Technology, is a high-resolution particle size analyser that uses the industry standard sedimentation method.
Manufacturer Micromeritics
Product Series SediGraph, a Micromeritics Technology
Measurement principle Sedimentation
Application Density, pore size and volume, Particle Mass and Concentration, Particle Size, Surface Area & Porosity
Particle size range 300 to 0.1 micrometers Equivalent Spherical Diameter
Sample Size 50 mL of dispersed sample – precise concentration is not required
Suspending Liquids Any liquid compatible with sample cell materials and not highly absorptive of Xrays (typical liquids are water, glycols, mineral oils, SediSperse®, and alcohols)
Temperature Ambient +10 to 40 °C

The SediGraph III Plus, a Micromeritics Technology, is a high-resolution particle size analyser capable of measuring particles from 300 to 0.1 micrometers. For over 50 years, Sedigraph continues to be the worldwide standard in particle size analysis for many industries, including mining, geology, and ceramics.

Sedigraph determines particle size by sedimentation by measuring the gravity-induced settling rates of different size particles in a liquid with known properties as described by Stokes’ Law. Particle mass is measured directly via X-ray absorption. This is a direct measurement; no calibration against reference material or modelling is required. The SediGraph is the only automated particle sizing instrument that directly measures settling velocity. The optional autosampler can run up to 18 samples unattended. It sits securely on top of the SediGraph to conserve bench space and completes most analyses in 15 min or less.

SediGraph uses a modern pumping system that is silent, reliable, and easy to maintain while the temperature-controlled mixing chamber improves repeatability and reproducibility. A highly versatile and interactive reporting system provides a wide range of custom data presentation options.

Resources

  • Entire introduced sample is accounted for including any fraction above 300 μm and below 0.1 μm
  • Merge data with other particle sizing methods, extending the range of reported data to 125,000 μm (125 mm), excellent for geological applications
  • Scans the sedimentation cell from bottom to top to allow accurate inventory of fast-settling particles while minimising the time required to resolve the separation of fine particles
  • Fully automatic operation increases sample throughput and reduces operator involvement and the opportunity for human error
  • Temperature-controlled analyses ensure liquid properties remain constant throughout the analysis
  • Multiple analysis speeds enables choice of the desired combination of speed and resolution that meets your needs
  • Real-Time display monitors the cumulative mass plot of the current analysis to allow immediate procedural changes if needed
  • Statistical process control (SPC) reports track the performance of processes allowing immediate response to fluctuations
  • Plot overlays provide a visual comparison of analysis results from one or more analyses; e.g. a reference or baseline analysis
  • Data comparison plots provide graphical displays of the mathematical difference between two data sets (difference from reference plot) or the extent of a data point value above or below a tolerance boundary (out of specification plot)
  • Multiple analyser control allows two SediGraphs to be operated simultaneously from a single computer, conserving valuable lab space and optimise data storage.

Ceramics: The size range of particles and the distribution of mass in each size class strongly affect the ability to sinter a ceramic powder and it’s forming properties as well as the pore size distribution in the finished product. Particle size distribution information helps to determine curing and bonding procedures, control pore structure, ensure adequate green body strength, and produce a final product of desired strength, texture, appearance, and density.

Metal Powders: By controlling particle size, very specific pore characteristics can be designed into a product. Porosity characteristics often are the key to product performance. Similar to ceramics, the particle size distribution is critical to green body and final product strength and density.

Geological/Soil Science: Grain Size affects the moisture-holding capacity of soil, drainage rate, and the soil’s ability to hold nutrients. Grain size is directly related to transport of sediment.

Cosmetics: The appearance, application, and packaging of cosmetics are influenced by the particle size distribution of base powders, such as talc, and the pigments used for coloring.

Pigments: Particle size alone can affect the tinting strength of a color. As tinting strength goes up, the quantity of pigment needed to produce required color intensity goes down. The particle size affects the hiding power of the paints. Also the particle size distribution influences gloss, texture, color saturation and brightness.

Catalysts: Particle size affects the catalytic activity of a metal for structure-sensitive catalytic reactions.

Construction Materials: Particle size of cement affects setting time and strength characteristics of finished concrete and cement.

Minerals and Inorganic Chemicals: Reactivity of materials is dependent upon exposed surface area and thus particle size distribution.

Abrasives: A properly balanced size distribution of abrasive grains and powders is a fundamental consideration whether the material is to be used in slurries, dry blasting, or bonded abrasive tools. Uniform particle size assures precise flow rates through blast machines and is a critical determination in media management when recycling the abrasive material.

High throughput with optional MasterTech autosampler

For automatic sample preparation. Redisperses samples and transfers them to the SediGraph for analysis. Includes built-in mechanical stirrer and ultrasonic probe.

What is the SediGraph used for?

The SediGraph measures particle size distributions of powders and suspensions by determining particle settling rates in a liquid. It is particularly effective for particles in the submicron to hundreds of microns size range.

How does the SediGraph measure particle size?

The instrument uses X-ray absorption to monitor the concentration of particles as they settle through a liquid. Particle size is calculated based on settling velocity using Stokes’ Law.

What particle size range can the SediGraph measure?

Depending on the model and sample properties, the SediGraph can typically measure particles from approximately 0.1 µm to 300 µm.

What types of materials can be analysed?

The SediGraph is suitable for a wide range of materials, including minerals, ceramics, pigments, catalysts, battery materials, pharmaceuticals, cement, and industrial powders.

Which industries commonly use the SediGraph?

The SediGraph is widely used in mining, minerals processing, cement production, battery manufacturing, advanced materials, chemicals, pharmaceuticals, and academic research laboratories.

What sample preparation is required?

Samples are dispersed in a suitable liquid medium using mechanical stirring, sonication, dispersants, or other methods to achieve a stable suspension before analysis.

How long does a typical analysis take?

Analysis times vary depending on the particle size range being measured, but most measurements can be completed within 15 minutes to a few hours.

Can I have a demonstration of the Sedigraph?

Yes, if a system is available. Contact us for a booking. We can arrange a personalised demo and test your samples within our lab facility in Sydney. Contact us for a demo.

SediGraph III Plus, Micromeritics technology

Customer installations

Imerys

SediGraph III Plus, Micromeritics technology

Imerys has recently installed their new Micromeritics Sedigraph system. Imerys is a world leading supplier of mineral-based specialty solutions for industry. The Sedigraph will help deliver high value-added functional solutions to a number of sectors from processing industries to consumer goods. Particle size distribution information will help to determine curing and bonding procedures, control pore structure, ensure adequate green body strength, and produce a final product of desired strength, texture, appearance, and density.

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